Gravimetric sorption is a popular analytical method utilized for the determination of the rate of interaction between a gas and an either solid or liquid material. The gravimetric sorption technique works with a sample’s weight being continuously measured on a microbalance as gas pressure is modulated under a constant temperature. Sorption update is established based on the measured changes of weight.
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| Company | Hiden Isochema | Hiden Isochema | Hiden Isochema | Hiden Isochema |
| Item | IMI-HTP Hydrogen Storage Analyzer | IGA-003 Dynamic Gas Sorption Analyzer | IGA-003-MC Binary Gas Sorption Analyzer | IMI-PSI High Pressure Manometric Sorption Analyzer |
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| Catalog Number | IMI-HT | IGA-003 | IGA-003-MC | IMI-PSI |
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| Temperature Range | 77 K to 500 °C | 77 K to 1000 °C | Inquire | 77 K to 773 K |
| Pressure Range | 100 bar (standard) 200 bar (optional) | 10 bar (standard) 20 bar (optional) | 0.5 to 3 bar | 100 bar (standard) 200 bar (optional) |
| Description | The IMI-HTP is designed to characterize hydrogen storage materials using Sieverts method up to pressures of 200 bar. High accuracy is ensured by a minimized dead volume, all-metal construction, high thermal stability and accurate pressure measurement. Every IMI-HTP is specified to meet the The IMI-HTP is designed to characterize hydrogen storage materials using Sieverts method up to pressures of 200 bar. High accuracy is ensured by a minimized dead volume, all-metal construction, high thermal stability and accurate pressure measurement. Every IMI-HTP is specified to meet the challenging demands of high pressure H2 operation, with permanent overpressure protection to satisfy the most rigorous safety requirements.
Features:
- Sub-microgram hydrogen sorption resolution
- High pressure operation from ambient temperature to 773 K
- Liquid N2 coolant options for low temperature physisorption
- Fully upgradable modular design
- Versatile instrument control, with fully programmable software
- Also operates with a range of other gases (N2, CH4, CO2, O2,…)
... Read More | The IGA-003 is a dynamic gas sorption analyzer incorporating multiple controllable inlets with combined pressure and flow control, and integrated mass spectrometry. Incorporating an ultra-sensitive microbalance, the IGA-003 measures changes in sample mass as a function of temperature, pressure and The IGA-003 is a dynamic gas sorption analyzer incorporating multiple controllable inlets with combined pressure and flow control, and integrated mass spectrometry. Incorporating an ultra-sensitive microbalance, the IGA-003 measures changes in sample mass as a function of temperature, pressure and gas composition. The unique IGA method analyzes real time gravimetric data to determine kinetic parameters and simultaneously predict sorption equilibrium.
Features:
- Fully programmable with combined control of pressure, flow and gas composition
- Optional integrated vapor generator module
- Sample temperatures from 77 K to 1000 °C
- Fully programmable for advanced method development
- Fully integrated quadrupole mass spectrometry option for evolved gas analysis (EGA)
... Read More | The IGA-003-MC is a gravimetric sorption analyzer for binary gas sorption analysis using the IMB (Integral Mass Balance) analysis technique. The IMB method allows binary gas adsorption isotherms to be measured by combining the controlled flow of a gas mixture with in situ gravimetric measurement andThe IGA-003-MC is a gravimetric sorption analyzer for binary gas sorption analysis using the IMB (Integral Mass Balance) analysis technique. The IMB method allows binary gas adsorption isotherms to be measured by combining the controlled flow of a gas mixture with in situ gravimetric measurement and outlet gas composition analysis using a mass spectrometer.
Features:
- Dynamic mode gas delivery with gas flow calibration
- Dedicated sample reactor with combi bath / heater for sample thermostatting
- Optimized sampling interface with a close-coupled Hiden mass spectrometer
- Recommended sample size is 3.5 grams for operation in the pressure range 0.5 bar to 3 bar
- Unique IMB method for partial uptake determination
... Read More | The IMI-PSI is designed to investigate gas sorption by nanoporous materials, from sub-ambient pressures to 200 bar. Its inherent flexibility allows both BET surface area analysis and gas storage studies to be performed using only one instrument, while an optimized design and superior build quality The IMI-PSI is designed to investigate gas sorption by nanoporous materials, from sub-ambient pressures to 200 bar. Its inherent flexibility allows both BET surface area analysis and gas storage studies to be performed using only one instrument, while an optimized design and superior build quality ensures high accuracy. Full automation enables pre-programmed gas switching and sample pretreatment routines to be set for ease-of-use.
Features:
- Sub-micromole gas sorption resolution
- 200 bar operation, with 773 K degassing capability
- Liquid coolant thermostatting, including LN2 for BET analysis
- Enhanced low pressure measurement accuracy
- Fully upgradable modular design
... Read More |
| Applications | Hydrogen storage capacity determination, Pressure-Composition-Temperature (PCT) measurements, Thermodynamic and kinetic studies, Metal hydrides and nanoporous materials (carbons, zeolites, MOFs and polymers) | Energy storage, Temperature Programmed Desorption/Oxidation/Reduction (TPD/TPO/TPR), Gas adsorption capacity determination, Thermodynamic and kinetic studies, Evolved Gas Analysis (EGA) and Thermogravimetric Analysis (TGA) | Inquire | Gas adsorption isotherm determination, Specific surface area (BET) determination, Energy gas (H2, CH4) storage and separation, Thermodynamics of high pressure gas adsorption, Nanoporous materials (carbons, zeolites, MOFs, polymers and shales) |
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