Gravimetric sorption is a popular analytical method utilized for the determination of the rate of interaction between a gas and an either solid or liquid material. The gravimetric sorption technique works with a sample’s weight being continuously measured on a microbalance as gas pressure is modulated under a constant temperature. Sorption update is established based on the measured changes of weight.
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| Company | Hiden Isochema | Hiden Isochema | Hiden Isochema | Hiden Isochema |
| Item | IMI-FLOW Manometric Gas Sorption Analyzer | IGA-003-MC Binary Gas Sorption Analyzer | IGA-1000 Advanced Gravimetric Sorption Analyzer | IMI-HTP Hydrogen Storage Analyzer |
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| Catalog Number | IMI-FLOW | IGA-003-MC | IGA-100 | IMI-HT |
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| Temperature Range | 77 K to 773 K | Inquire | 77 K to 1000 °C | 77 K to 500 °C |
| Pressure Range | 100 bar (standard) 200 bar (optional) | 0.5 to 3 bar | 10 bar (standard) 20 bar (optional) | 100 bar (standard) 200 bar (optional) |
| Description | The IMI-FLOW combines the manometric gas sorption capabilities of all IMI analyzers with flowing mode operation and integrated mass spectrometry. Manometric mode offers high accuracy isotherm determination to 200 bar, while the flowing mode provides complete control of pressure, composition and flowThe IMI-FLOW combines the manometric gas sorption capabilities of all IMI analyzers with flowing mode operation and integrated mass spectrometry. Manometric mode offers high accuracy isotherm determination to 200 bar, while the flowing mode provides complete control of pressure, composition and flow rate. Integrated mass spectrometry allows downstream gas analysis for TPD and advanced methods.
Features:
- Sub-micromole gas sorption resolution
- High pressure operation from 77 K to 773 K
- Automatic switching between manometric and flowing mode operation
- Versatile control from standard methods to complete user-defined experiments
- Full integration of mass spectrometers from Hiden’s quadrupole range
... Read More | The IGA-003-MC is a gravimetric sorption analyzer for binary gas sorption analysis using the IMB (Integral Mass Balance) analysis technique. The IMB method allows binary gas adsorption isotherms to be measured by combining the controlled flow of a gas mixture with in situ gravimetric measurement andThe IGA-003-MC is a gravimetric sorption analyzer for binary gas sorption analysis using the IMB (Integral Mass Balance) analysis technique. The IMB method allows binary gas adsorption isotherms to be measured by combining the controlled flow of a gas mixture with in situ gravimetric measurement and outlet gas composition analysis using a mass spectrometer.
Features:
- Dynamic mode gas delivery with gas flow calibration
- Dedicated sample reactor with combi bath / heater for sample thermostatting
- Optimized sampling interface with a close-coupled Hiden mass spectrometer
- Recommended sample size is 3.5 grams for operation in the pressure range 0.5 bar to 3 bar
- Unique IMB method for partial uptake determination
... Read More | The IGA-100 is an advanced gravimetric sorption analyzer, powerfully combining high resolution vapor, mixed gas and TGA-MS measurements. A multiple inlet flow control system allows mixed gas experiments with combined pressure, flow and composition control, while anti-condensation protection and The IGA-100 is an advanced gravimetric sorption analyzer, powerfully combining high resolution vapor, mixed gas and TGA-MS measurements. A multiple inlet flow control system allows mixed gas experiments with combined pressure, flow and composition control, while anti-condensation protection and active pressure regulation enable high resolution vapor sorption-desorption measurements.
Features:
- Fully programmable with combined control of pressure, flow and gas composition
- Built-in anti-condensation protection to 50 °C for pure vapor sorption
- Optional integrated vapor generator module for dynamic vapor sorption (DVS)
- Sample temperatures from 77 K to 1000 °C
- Fully integrated quadrupole mass spectrometry option for evolved gas analysis (EGA)
- Unique combination of vapor sorption options to include DVS measurements with pressure and vacuum control
... Read More | The IMI-HTP is designed to characterize hydrogen storage materials using Sieverts method up to pressures of 200 bar. High accuracy is ensured by a minimized dead volume, all-metal construction, high thermal stability and accurate pressure measurement. Every IMI-HTP is specified to meet the The IMI-HTP is designed to characterize hydrogen storage materials using Sieverts method up to pressures of 200 bar. High accuracy is ensured by a minimized dead volume, all-metal construction, high thermal stability and accurate pressure measurement. Every IMI-HTP is specified to meet the challenging demands of high pressure H2 operation, with permanent overpressure protection to satisfy the most rigorous safety requirements.
Features:
- Sub-microgram hydrogen sorption resolution
- High pressure operation from ambient temperature to 773 K
- Liquid N2 coolant options for low temperature physisorption
- Fully upgradable modular design
- Versatile instrument control, with fully programmable software
- Also operates with a range of other gases (N2, CH4, CO2, O2,…)
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| Applications | Gas storage, Gas separation and purification, Thermodynamic and kinetic studies, Nanoporous materials (carbons, zeolites, MOFs and polymers) | Inquire | Gas adsorption capacity determination, Moisture and organic vapor sorption, Catalyst characterization, Moisture and organic vapor sorption with diffusion coefficient determination, Thermogravimetric Analysis (TGA) and Evolved Gas Analysis (EGA), Temperature Programmed Desorption/Oxidation/Reduction (TPD, TPO, TPR) | Hydrogen storage capacity determination, Pressure-Composition-Temperature (PCT) measurements, Thermodynamic and kinetic studies, Metal hydrides and nanoporous materials (carbons, zeolites, MOFs and polymers) |
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