X-ray diffraction (XRD) allows one to ascertain the molecular structure of a crystalline material by diffracting X-rays through the sample. An XRD analyzer obtains interference patterns reflecting lattice structures by varying the angle of incidence of the X-ray beam. Thus, the precision, speed of rotation, and beam size of the X-rays become important parameters by which to judge products. Benchtop XRD can be targeted for single crystal diffraction for imaging lattices; powder diffraction for phase determination; identifying unfamiliar substances for use in inspection, crystallography, and pharmaceutical research correlating crystal structures with drug efficacy. X-ray generators can reach 18 KW in power and detectors typically come as compound silicon arrays, Peltier-Cooled, Silicon Drift, or Scintillation Counter variants. Software targeted for specific XRD applications is available for upgrade in some analyzer models.
Find, compare, and request a quote for X-ray diffractometers (XRD instruments) across leading suppliers at Labcompare; including access to product citations, related published figures, and first-hand reviews from our scientific community.
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| Company | Rigaku Corporation | Rigaku Corporation | Rigaku Corporation | Rigaku Corporation | Rigaku Corporation |
| Item | SmartLab High-Resolution Diffraction System | AutoMATE II | Miniflex XpC XRD | Rigaku XtaLAB Synergy Flow Automated Single Crystal XRD | XtaLAB Synergy-Custom |
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| Catalog Number | SmartLab | AutoMATE II | MiniFlex XpC | | XtaLAB Synergy-Custom |
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| X-Ray Tube | 3 kW sealed X-ray tube | Cr (Maximum load 2 kW), Effective focus size 1 × 10 mm2 (N.F.), Short type | 600 W | Inquire | Inquire |
| X-Ray Generator | 9.0 kW Rotating Anode Generator | 3 kW sealed X-ray tube | Compact 800 W generator and compact X-ray tube | Inquire | MicroMax-007 HF microfocus rotating anode source or the highest-flux in-house X-ray source, the FR-X (Mo, Cu, or Cr). |
| Goniometer Type | High Resolution Theta/Theta Closed Loop | two-axis goniometer | Θ-Θ sample horizontal goniometer | Intelligent Goniometer Head (IGH) with motorized automation; automated sample centering in as little as 6 seconds | Fast kappa geometry goniometer |
| Detector(s) | D/teX Ultra 250 silicon strip detector | D/teX Ultra 1000 | D/teX Ultra silicon strip | Direct X-ray detection detectors (varies by Synergy base model selected) | HyPix-6000HE, the large theta coverage HyPix-Arc 150° or the Dectris EIGER 4M. |
| Description | The SmartLab high-resolution diffraction system represents the state of the art in fully automated modular XRD systems. The system incorporates a high resolution theta/theta closed loop goniometer drive system, CBO, an in-plane scattering arm, an optional 9.0 kW rotating anode generator, and a fullyThe SmartLab high-resolution diffraction system represents the state of the art in fully automated modular XRD systems. The system incorporates a high resolution theta/theta closed loop goniometer drive system, CBO, an in-plane scattering arm, an optional 9.0 kW rotating anode generator, and a fully automated optical system to make advanced measurements possible for both expert and novice users of the system.
Winner of the 2006 R&D 100 Award for technical innovation, the SmartLab is design for completely automated analysis of thin films and other advanced materials. Powered by Guidance, Rigaku's revolutionary knowledge based software package, SmartLab uses fully deveopled measurement packages for completely automated measurement of thin films, nanomaterials, powders, and liquids. Measurement packages exist for powder diffraction, glancing incidence diffraction, in-plane diffraction, X-ray reflectivity, and small angle X-ray scattering (SAXS) measurements.
Features - Θ/Θ design for horizontal sample mounting
- Closed loop drive system for high resolution scanning
- Optional 9.0 kW rotating anode generator
- Fully automatic system alignment
- Guidance software based automated measurement
- 300 mm wafer handling
- CBO for focusing and parallel beam geometries without reconfiguration
- In-plane diffraction arm for in-plane measurements without reconfiguration
- High resolution optics
- SAXS capabilities
... Read More | The AutoMATE II can measure large and heavy parts (30 kg with standard manual Z stage; 20 kg with optional automated XYZ stage) with high accuracy.
The X-ray source and detector arm are mounted on a highly accurate two-axis goniometer that can position them relative to the measurement site and The AutoMATE II can measure large and heavy parts (30 kg with standard manual Z stage; 20 kg with optional automated XYZ stage) with high accuracy.
The X-ray source and detector arm are mounted on a highly accurate two-axis goniometer that can position them relative to the measurement site and perform scans with minimum steps of 0.1 microns when using the automated XYZ stage.
Features: - Highly accurate goniometer allows for true micro-area residual stress measurement.
- Automatic mapping measurements with teaching function.
- An X-ray radiation enclosure with interlock system automatically locks the enclosure door when the X-ray shutter is open.
- The measurement position is adjusted by _x000B_a CCD camera equipped with a microscope having a zoom function.
- The two-axis goniometer system allows for both iso-inclination _x000B_and side-inclination methods automatically without readjustment of the sample position.
... Read More | The Miniflex XpC is an X-ray diffractometer designed specifically for quality control in cement plants and other operations requiring online process control such as pharmaceuticals and batteries. It has been optimized for speed and accuracy, bringing lab-quality performance to the manufacturing The Miniflex XpC is an X-ray diffractometer designed specifically for quality control in cement plants and other operations requiring online process control such as pharmaceuticals and batteries. It has been optimized for speed and accuracy, bringing lab-quality performance to the manufacturing floor.
With this in mind, the MiniFlex XpC allows you to process more samples faster, and to gain greater control over your process to ensure consistent quality of your final product. The system is characterized by streamlined operation, rapid analysis with pass/fail evaluation and the ability to automate and integrate with other complementary analytical instruments. The MiniFlex XpC offers the performance level of much larger systems, in the world’s smallest footprint for an online XRD.
Features: Analytical speed and accuracy are paramount in industrial operations. These factors have been addressed in the design of the MiniFlex XpC by using: - A newly design compact, 800 W high-flux X-ray source and power supply
- World’s largest area/high-throughput 1D detector, enabling higher-intensity data collection
- Optimized θ / θ sample geometry that maintains a horizontal sample orientation
- Streamlined user interface
- Compatibility with sample loading robots or conveyors
- Compact design that can easily be incorporated into existing operations
- A recently patented variable-width scattering slit minimizing background at lower angles
- Sample spinner that negates the effects of preferred orientation
- Uses industry standard steel ring sample holders
Streamlined Operation In addition to sample loading automation, Rigaku has introduced EasyX, a simplified user interface that allows operators of any skill level to measure and obtain results in as few as three clicks. Built on the same comprehensive platform that underpins Rigaku’s most sophisticated XRDs like the SmartLab, EasyX provides simplified access to the functionalities required for routine QC workflows, including automated pass/fail analysis. A user-friendly graphical user interface accessible via the optional touchscreen allows simple operation of the instrument as well as interpretation of the results.
Compact Design The MiniFlex XpC has the smallest footprint (0.9 m2) of any instrument in its class. This specification includes the touchscreen user interface.
Online Quality Control A newly developed sample loader makes the MiniFlex XpC ideal for QC operations. For applications with higher-throughput levels, the system can be integrated with a sample loading robot or a conveyor.... Read More | Inquire | Customized Single Crystal Diffraction System With Microfocus Rotating Anode Generator
Features: - Ultimate flexibility with customized X-ray system specifically tailored to the needs of your research. Dual ports allow for various combinations of crystallography and SAXS configurations. Your choice
Customized Single Crystal Diffraction System With Microfocus Rotating Anode Generator
Features: - Ultimate flexibility with customized X-ray system specifically tailored to the needs of your research. Dual ports allow for various combinations of crystallography and SAXS configurations. Your choice of VariMax™ confocal double-bounce optics for better spectral purity and beam size to match your sample types.
- Faster, accurate data collection due to high-speed kappa goniometer, high-flux rotating anode X-ray source, fast, low-noise X-ray detector, and highly optimized instrument control software.
- Improve your ability to investigate small samples due to the increased flux from the rotating anode X-ray source as well as the extreme low noise of the HyPix X-ray detectors. Noise-free images mean you can count longer for weakly diffracting crystals without a loss in data quality arising from detector noise.
- Screen crystals in situ with optional XtalCheck crystallization plate screening device.
- Enhance your ability to resolve large unit cells, twins or incommensurate lattices when you select the optional motorized variable beam slit in order to alter divergence to adapt the source to your sample’s requirements.
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