X-ray diffraction (XRD) allows one to ascertain the molecular structure of a crystalline material by diffracting X-rays through the sample. An XRD analyzer obtains interference patterns reflecting lattice structures by varying the angle of incidence of the X-ray beam. Thus, the precision, speed of rotation, and beam size of the X-rays become important parameters by which to judge products. Benchtop XRD can be targeted for single crystal diffraction for imaging lattices; powder diffraction for phase determination; identifying unfamiliar substances for use in inspection, crystallography, and pharmaceutical research correlating crystal structures with drug efficacy. X-ray generators can reach 18 KW in power and detectors typically come as compound silicon arrays, Peltier-Cooled, Silicon Drift, or Scintillation Counter variants. Software targeted for specific XRD applications is available for upgrade in some analyzer models.
Find, compare, and request a quote for X-ray diffractometers (XRD instruments) across leading suppliers at Labcompare; including access to product citations, related published figures, and first-hand reviews from our scientific community.
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| Company | Rigaku Corporation | Rigaku Corporation | Rigaku Corporation | Rigaku Corporation | Rigaku Corporation |
| Item | DicifferX WAXS Edition | Miniflex XpC XRD | Rigaku XtaLAB Synergy Flow Automated Single Crystal XRD | XtaLAB Synergy-Custom | XtaLAB Synergy-ED Electron Diffractometer |
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| Catalog Number | | MiniFlex XpC | | XtaLAB Synergy-Custom | XtaLAB Synergy-ED |
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| X-Ray Tube | Inquire | 600 W | Inquire | Inquire | Inquire |
| X-Ray Generator | High-brilliance rotating anode with multilayer focusing mirror (10^9 cps at 200 µm beam) | Compact 800 W generator and compact X-ray tube | Inquire | MicroMax-007 HF microfocus rotating anode source or the highest-flux in-house X-ray source, the FR-X (Mo, Cu, or Cr). | Inquire |
| Goniometer Type | No goniometer (open stage design) | Θ-Θ sample horizontal goniometer | Intelligent Goniometer Head (IGH) with motorized automation; automated sample centering in as little as 6 seconds | Fast kappa geometry goniometer | Single rotation axis |
| Detector(s) | HyPix-6000 2D HPAD on motorized 2-axis stage | D/teX Ultra silicon strip | Direct X-ray detection detectors (varies by Synergy base model selected) | HyPix-6000HE, the large theta coverage HyPix-Arc 150° or the Dectris EIGER 4M. | High-speed, high-sensitivity photon-counting detector, HyPix-ED |
| Description | Inquire | The Miniflex XpC is an X-ray diffractometer designed specifically for quality control in cement plants and other operations requiring online process control such as pharmaceuticals and batteries. It has been optimized for speed and accuracy, bringing lab-quality performance to the manufacturing The Miniflex XpC is an X-ray diffractometer designed specifically for quality control in cement plants and other operations requiring online process control such as pharmaceuticals and batteries. It has been optimized for speed and accuracy, bringing lab-quality performance to the manufacturing floor.
With this in mind, the MiniFlex XpC allows you to process more samples faster, and to gain greater control over your process to ensure consistent quality of your final product. The system is characterized by streamlined operation, rapid analysis with pass/fail evaluation and the ability to automate and integrate with other complementary analytical instruments. The MiniFlex XpC offers the performance level of much larger systems, in the world’s smallest footprint for an online XRD.
Features:
Analytical speed and accuracy are paramount in industrial operations. These factors have been addressed in the design of the MiniFlex XpC by using: - A newly design compact, 800 W high-flux X-ray source and power supply
- World’s largest area/high-throughput 1D detector, enabling higher-intensity data collection
- Optimized θ / θ sample geometry that maintains a horizontal sample orientation
- Streamlined user interface
- Compatibility with sample loading robots or conveyors
- Compact design that can easily be incorporated into existing operations
- A recently patented variable-width scattering slit minimizing background at lower angles
- Sample spinner that negates the effects of preferred orientation
- Uses industry standard steel ring sample holders
Streamlined Operation
In addition to sample loading automation, Rigaku has introduced EasyX, a simplified user interface that allows operators of any skill level to measure and obtain results in as few as three clicks. Built on the same comprehensive platform that underpins Rigaku’s most sophisticated XRDs like the SmartLab, EasyX provides simplified access to the functionalities required for routine QC workflows, including automated pass/fail analysis. A user-friendly graphical user interface accessible via the optional touchscreen allows simple operation of the instrument as well as interpretation of the results.
Compact Design
The MiniFlex XpC has the smallest footprint (0.9 m2) of any instrument in its class. This specification includes the touchscreen user interface.
Online Quality Control
A newly developed sample loader makes the MiniFlex XpC ideal for QC operations. For applications with higher-throughput levels, the system can be integrated with a sample loading robot or a conveyor.... Read More | Inquire | Customized Single Crystal Diffraction System With Microfocus Rotating Anode Generator
Features: - Ultimate flexibility with customized X-ray system specifically tailored to the needs of your research. Dual ports allow for various combinations of crystallography and SAXS configurations. Your choice
Customized Single Crystal Diffraction System With Microfocus Rotating Anode Generator
Features: - Ultimate flexibility with customized X-ray system specifically tailored to the needs of your research. Dual ports allow for various combinations of crystallography and SAXS configurations. Your choice of VariMax™ confocal double-bounce optics for better spectral purity and beam size to match your sample types.
- Faster, accurate data collection due to high-speed kappa goniometer, high-flux rotating anode X-ray source, fast, low-noise X-ray detector, and highly optimized instrument control software.
- Improve your ability to investigate small samples due to the increased flux from the rotating anode X-ray source as well as the extreme low noise of the HyPix X-ray detectors. Noise-free images mean you can count longer for weakly diffracting crystals without a loss in data quality arising from detector noise.
- Screen crystals in situ with optional XtalCheck crystallization plate screening device.
- Enhance your ability to resolve large unit cells, twins or incommensurate lattices when you select the optional motorized variable beam slit in order to alter divergence to adapt the source to your sample’s requirements.
... Read More | The XtaLAB Synergy-ED is the world’s first 3DED/microED (3D Electron Diffraction/micro Electron Diffraction) system and the successful culmination of a joint development project between Rigaku and JEOL. 3DED/microED allows crystallographers to probe the structure of crystals and The XtaLAB Synergy-ED is the world’s first 3DED/microED (3D Electron Diffraction/micro Electron Diffraction) system and the successful culmination of a joint development project between Rigaku and JEOL. 3DED/microED allows crystallographers to probe the structure of crystals and nanocrcrystals as small as tens of nanometers, opening up many new possibilities. This new capability allows you to go beyond the limitations of X-ray diffraction (XRD), which requires samples greater them 1 µm.
- Directly determine 3D molecular structures of submicron crystals for the first time
- Rigaku’s high-speed, high-sensitivity photon counting detector - HyPix-ED
- JEOL’s expertise in generation and control of stable electron beams – 200 kV electron source and optics
- Rigaku’s powerful single crystal analysis software – CrysAlisPro-ED
3DED/microED is an excellent complementary technique to XRD, and the compact design of the XtaLAB Synergy-ED allows it to be easily located in laboratories alongside these instruments. Crystallographers familiar with Rigaku diffractometers running CrysAlisPRO will be able to adapt to the CrysAlisPRO-ED interface very quickly, as it is based on the same intuitive platform.
The fully integrated system incorporates a seamless workflow from data collection to structure determination of three-dimensional molecular structures. AutoChem, which is fully integrated into CrysAlisPRO, performs fast, fully automated structure solution and refinement during data collection, optimizing your productivity.
3DED/microED allows direct structural determination of sub-micron sized crystals that could only previously be postulated by techniques such as NMR. As an emerging technique, there is scope for the generation of many publications using the XtaLAB Synergy-ED.
... Read More |
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