X-ray diffraction (XRD) allows one to ascertain the molecular structure of a crystalline material by diffracting X-rays through the sample. An XRD analyzer obtains interference patterns reflecting lattice structures by varying the angle of incidence of the X-ray beam. Thus, the precision, speed of rotation, and beam size of the X-rays become important parameters by which to judge products. Benchtop XRD can be targeted for single crystal diffraction for imaging lattices; powder diffraction for phase determination; identifying unfamiliar substances for use in inspection, crystallography, and pharmaceutical research correlating crystal structures with drug efficacy. X-ray generators can reach 18 KW in power and detectors typically come as compound silicon arrays, Peltier-Cooled, Silicon Drift, or Scintillation Counter variants. Software targeted for specific XRD applications is available for upgrade in some analyzer models.
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| Company | Rigaku Corporation | Rigaku Corporation | Rigaku Corporation | Rigaku Corporation |
| Item | LabLinc Studio Modular Integration platform for Autonomous Labs | AutoMATE II | Rigaku XtaLAB Synergy Flow Automated Single Crystal XRD | SmartLab High-Resolution Diffraction System |
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| Catalog Number | LabLinc Studio | AutoMATE II | | SmartLab |
| Price | | | | |
| X-Ray Tube | Inquire | Cr (Maximum load 2 kW), Effective focus size 1 × 10 mm2 (N.F.), Short type | Inquire | 3 kW sealed X-ray tube |
| X-Ray Generator | Inquire | 3 kW sealed X-ray tube | Inquire | 9.0 kW Rotating Anode Generator |
| Goniometer Type | Inquire | two-axis goniometer | Intelligent Goniometer Head (IGH) with motorized automation; automated sample centering in as little as 6 seconds | High Resolution Theta/Theta Closed Loop |
| Detector(s) | Inquire | D/teX Ultra 1000 | Direct X-ray detection detectors (varies by Synergy base model selected) | D/teX Ultra 250 silicon strip detector |
| Description | LabLinc Studio is Rigaku’s modular integration offering for autonomous labs, combining RAI (Rigaku Automation Interface), SmartLab software workflow packaging, and optional automation hardware (sample handling, robots, robot-compatible doors/enclosures) plus technical support. Critical instrument LabLinc Studio is Rigaku’s modular integration offering for autonomous labs, combining RAI (Rigaku Automation Interface), SmartLab software workflow packaging, and optional automation hardware (sample handling, robots, robot-compatible doors/enclosures) plus technical support. Critical instrument settings are exposed through Python API for easy integration of analytical instruments into autonomous labs and AI-driven materials discovery loop.... Read More | The AutoMATE II can measure large and heavy parts (30 kg with standard manual Z stage; 20 kg with optional automated XYZ stage) with high accuracy.
The X-ray source and detector arm are mounted on a highly accurate two-axis goniometer that can position them relative to the measurement site and The AutoMATE II can measure large and heavy parts (30 kg with standard manual Z stage; 20 kg with optional automated XYZ stage) with high accuracy.
The X-ray source and detector arm are mounted on a highly accurate two-axis goniometer that can position them relative to the measurement site and perform scans with minimum steps of 0.1 microns when using the automated XYZ stage.
Features: - Highly accurate goniometer allows for true micro-area residual stress measurement.
- Automatic mapping measurements with teaching function.
- An X-ray radiation enclosure with interlock system automatically locks the enclosure door when the X-ray shutter is open.
- The measurement position is adjusted by _x000B_a CCD camera equipped with a microscope having a zoom function.
- The two-axis goniometer system allows for both iso-inclination _x000B_and side-inclination methods automatically without readjustment of the sample position.
... Read More | Inquire | The SmartLab high-resolution diffraction system represents the state of the art in fully automated modular XRD systems. The system incorporates a high resolution theta/theta closed loop goniometer drive system, CBO, an in-plane scattering arm, an optional 9.0 kW rotating anode generator, and a fullyThe SmartLab high-resolution diffraction system represents the state of the art in fully automated modular XRD systems. The system incorporates a high resolution theta/theta closed loop goniometer drive system, CBO, an in-plane scattering arm, an optional 9.0 kW rotating anode generator, and a fully automated optical system to make advanced measurements possible for both expert and novice users of the system.
Winner of the 2006 R&D 100 Award for technical innovation, the SmartLab is design for completely automated analysis of thin films and other advanced materials. Powered by Guidance, Rigaku's revolutionary knowledge based software package, SmartLab uses fully deveopled measurement packages for completely automated measurement of thin films, nanomaterials, powders, and liquids. Measurement packages exist for powder diffraction, glancing incidence diffraction, in-plane diffraction, X-ray reflectivity, and small angle X-ray scattering (SAXS) measurements.
Features - Θ/Θ design for horizontal sample mounting
- Closed loop drive system for high resolution scanning
- Optional 9.0 kW rotating anode generator
- Fully automatic system alignment
- Guidance software based automated measurement
- 300 mm wafer handling
- CBO for focusing and parallel beam geometries without reconfiguration
- In-plane diffraction arm for in-plane measurements without reconfiguration
- High resolution optics
- SAXS capabilities
... Read More |
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