X-Ray Fluorescence spectrometers (XRF) use high energy X-rays (or gamma rays) to excite fluorescent radiation or photons from a sample for elemental analysis. In wavelength dispersive x-ray fluorescence spectroscopy (WDXRF), photons emitted by the sample are separated or dispersed by diffraction before hitting the detector. This is accomplished by placing an analyzing crystal between the sample and the detector. Therefore, WDXRF spectrometers have better resolution than energy dispersive x-ray fluorescence spectrometers which do not contain an analyzing crystal. However, due to the increase in optical components, WDXRF spectrometers typical have a lower efficiency than EDXRF spectrometers and, hence, require a higher power x-ray tube (which can add to the cost of the instrument).
There are two types of WDXRF spectrometers: simultaneous and sequential. In simultaneous WDXRF spectrometers, multiple detectors placed at different angles are used to analyze multiple elements simultaneously. In sequential WDXRF Spectrometers, the crystal is turned while elements are analyzed sequentially. Sequential WDXRF spectrometers typically have better intensity, but take longer to record measurements. WDXRF is a nondestructive technique and has applications in many industries where elemental analysis is needed, such as geoscience, environmental analysis, food safety, and analyzing archeological artifacts.
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Energy Dispersive XRF Spectrometers (EDXRF)
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| Company | Rigaku Corporation | Rigaku Corporation |
| Item | Supermini200 High-Power Benchtop Sequential WDXRF Spectrometer | ZSX 400 Wavelength Dispersive X-ray Fluorescence Spectrometer |
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| Catalog Number | Supermini200 | ZSX 400 |
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| Principle | Wavelength dispersive X-ray fluorescence spectroscopy (WDXRF) | Wavelength Dispersive X-ray Fluorescence (WDXRF) |
| X-Ray Tube | 50 kV, 200 W Pd-anode | End window, Rh-anode, 3kW or 4 kW, 60kV |
| Goniometer Type | Inquire | Inquire |
| Detector(s) | Scintillation counter and F-PC (S-PC not requiring P10 gas optionally available) | Heavy element detector - Scintillation counter (SC), Light element detector - Flow proportional counter (F-PC), Attenuator - In-out automatic exchanger (1/10) |
| Analysis Diameter | Able to accommodate 51.5 mm diameter samples | 30 to 0.5 mm |
| Description | Elemental analysis of solids, liquids, powders, alloys and thin films
Compared to competing XRF systems, the Rigaku Supermini200 offers superior fundamental parameters and empirical software capabilities in a high resolution instrument with a compact footprint. As a high-power benchtop sequential Elemental analysis of solids, liquids, powders, alloys and thin films
Compared to competing XRF systems, the Rigaku Supermini200 offers superior fundamental parameters and empirical software capabilities in a high resolution instrument with a compact footprint. As a high-power benchtop sequential wavelength dispersive X-ray fluorescence (WDXRF) spectrometer, for elemental analysis of oxygen (O) through uranium (U) in almost any material, the Supermini200 uniquely delivers low cost-of-ownership (COO) with high resolution and lower limits-of-detection (LLD).
Features: - Analyze oxygen through uranium (O -> U)
- Analyze
Solids, liquids, powders, alloys and thin films - Atmosphere
Helium or vacuum - X-ray tube
50 kV, 200 W Pd-anode - Primary beam filter
Zr standard; Al optional - Detectors
Scintillation counter and F-PC (S-PC not requiring P10 gas optionally available) - Crystals
3-position changer - Sample size
Able to accommodate 51.5 mm diameter samples - Automatic sample changer (ASC)
Standard: 10 sample positions (for 51.5 mm diameter samples) Optional: 12 sample positions (up to 44mm diameter samples) - Vacuum
Rotary pump standard - Power
100 – 120V (50/60 Hz) 15A or 200 – 240V (50/60 Hz) 10A ... Read More | Rigaku's unique ZSX 400 sequential wavelength dispersive X-ray fluorescence (WDXRF) spectrometer was specifically designed to handle very large and/or heavy samples. Accepting samples up to 400 mm diameter, 50 mm thick and 30 kg weight, this system is ideal for analyzing sputtering targets, magneticRigaku's unique ZSX 400 sequential wavelength dispersive X-ray fluorescence (WDXRF) spectrometer was specifically designed to handle very large and/or heavy samples. Accepting samples up to 400 mm diameter, 50 mm thick and 30 kg weight, this system is ideal for analyzing sputtering targets, magnetic disks, or for multilayer film metrology or elemental analysis of large samples.
Customized sample adapter system Having the versatility to adapt to your specific sample types and analysis needs, the ZSX 400 is adaptable to various sample sizes and shapes using optional (made to order) adapter inserts. With a variable measurement spot (30 mm to 0.5 mm diameter with 5-step automatic selection) and mapping capability with multi-point measurements to check for sample uniformity, this uniquely flexible instrument can dramatically streamline your quality control processes.
Sample view camera with special lighting Optional real-time camera allows the analysis point to be viewed on screen. The operator has complete certainty as to what is being measured.
Traditional WDXRF analytical capabilities All analytical capabilities of a traditional instrument are retained in this "large sample" variant. Analyze beryllium (Be) through uranium (U) with high-resolution, high-precision WDXRF spectroscopy, from solids to liquids and powders to thin films. Analyze wide composition ranges (ppm to tens of percent) and thicknesses (sub Å to mm). Optionally available is diffraction peak interference rejection, for optimal results for single-crystal substrates. The Rigaku ZSX 400 complies with industry standards SEMI and CE.
Features - Large sample analysis
- Up to 400 mm (diameter)
- Up to 50 mm (thickness)
- Up to 30 kg (mass)
- Sample adapter system
- Adaptable to various sample sizes
- Measurement spot
- 30 mm to 0.5 mm diameter
- 5-step automatic selection
- Mapping capability
- Allows multipoint measurements
- Sample view camera (option)
- General purpose
- Analyze Be - U
- Elemental range: ppm to %
- Thickness range: sub Å to mm
- Diffraction interference rejection (option)
- Accurate results for single-crystal substrates
- Compliance with industry standards
- Small footprint
50% footprint of the previous model ... Read More |
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