This study used a workflow for broad scope suspect screening to identify toxic chemicals in wastewater effluents. The comprehensive approach combined targeted and untargeted methods using a high-resolution accurate mass Agilent 7250 GC/Q-TOF in multiple ionization modes, the GC/Q-TOF screening workflow in Agilent MassHunter Quantitative Analysis software 10.1, and the GC/Q-TOF accurate mass library of pesticides and environmental contaminants.

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