Description | The high-pressure DSC for specific reactions
Numerous physical processes and chemical reactions are influenced by the surrounding gas pressure. In practise it is therefore often necessary to conduct DSC measurements under an increased pressure.
With the high-pressure Differential Scanning Calorimeter,The high-pressure DSC for specific reactions
Numerous physical processes and chemical reactions are influenced by the surrounding gas pressure. In practise it is therefore often necessary to conduct DSC measurements under an increased pressure.
With the high-pressure Differential Scanning Calorimeter, DSC 204 HP Phoenix®, thermal effects in a sample can be analyzed in the pressure range from vacuum to 15 MPa (150 bar) and at temperatures from -150°C to 600°C, depending on the type of gas. The sample chamber atmosphere can be static or dynamic. The electronic pressure monitor and control, along with exact regulation of the purge gas flow, provide for excellent accuracy and reproducibility of the measurement results. The proven CC 200 L for liquid nitrogen cooling is available for the low-temperature range. The safety of the high-pressure DSC system has been certified through design tests and is guaranteed during operation by the appropriate safety components.... Read More | Studying Phase Transformations of Pharmaceuticals, Foods and Cosmetics by means of the DSC 214 Nevio the fastest heat-flux DSC instrument on the market.
Information obtained by differential scanning calorimetry (DSC):
- Melting temperatures and enthalpies
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Polymorphism
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Crystallization
Studying Phase Transformations of Pharmaceuticals, Foods and Cosmetics by means of the DSC 214 Nevio the fastest heat-flux DSC instrument on the market.
Information obtained by differential scanning calorimetry (DSC):
- Melting temperatures and enthalpies
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Polymorphism
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Crystallization temperatures and enthalpies
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Glass transitions
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Solid-solid interactions (e.g., compatibility)
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Phase diagrams
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Eutectic purity
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Solid-fat content
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Reaction temperatures and enthalpies
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Cross-linking reactions (curing)
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Oxidation-induction time and temperature (isothermal and dynamic OIT)
Features:
- Temperature range (max.): -170°C to 600°C
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Max. cooling rate/max. heating rate: 500 K/min
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Measuring range/ weighing range (max.): ± 750 mW
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Enthalpy accuracy: < 1% (for indium)
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TGA resolution: n/a
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Indium Response Ratio (*): > 100
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Exchangeable sensors: n/a
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Cooling options:
- Air compressor: RT to 600°C
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Compressed air: < 0°C to 600°C
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Intracooler: -70°C to 600°C
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Liquid nitrogen: -170°C to 700°C
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Gas atmospheres: Inert, oxidizing, static and dynamic
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Mass flow controller for purge/protective gas: 3, integrated (0 to 250 ml/min)
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Gas flow regulation: Software-controlled
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Automatic Sample Changer (ASC): Yes (optional)
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Software: min. Proteus® 8
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Proteus® software extensions included:
- SmartMode
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ExpertMode
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AutoCalibration
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(Advanced) BeFlat®
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AutoEvaluation
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Identify
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Proteus® software extensions (optional):
- Temperature modulation (not available in the USA)
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Specific heat capacity (cp)
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Proteus® Protect
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Purity Determination
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Advanced Software extensions (optional):
- Peak Separation
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Kinetics Neo
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Thermal Simulations
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Size (W x H x D) – incl. ASC, without physical connections: 350 mm x 445 mm x 560 mm
... Read More | The cost-effective starter instrument for material characterization
The DSC 3500 Sirius unites state-of-the-art technology with high sensitivity in a robust, easy-to-operate measuring system across a temperature range from -170°C to 600°C. The most important characteristics of the DSC 3500 Sirius The cost-effective starter instrument for material characterization
The DSC 3500 Sirius unites state-of-the-art technology with high sensitivity in a robust, easy-to-operate measuring system across a temperature range from -170°C to 600°C. The most important characteristics of the DSC 3500 Sirius measuring cell are its silver furnace with long-life heating element and its monolithic DSC sensor featuring high stability and optimal resolution.
For high sample throughput, we recommend that the unit be equipped with an automatic sample changer (ASC) – this accommodates up to 20 samples and references, even of different crucible types.
The design of the DSC 3500 Sirius developed in Japan is tailored to routine tasks in quality control and failure analysis as well as for material characterization of technical textiles, of food products, in packaging, in the polymer and cosmetic industry and for further organic or inorganic materials.... Read More | Fascinating Flexibility in Thermal Analysis
The DSC 404 F1 Pegasus® High-Temperature Differential Scanning Calorimeter, is designed for the exact determination of specific heat of high-performance materials at high temperatures.
- Determination of thermodynamic properties of ceramics and metallic
Fascinating Flexibility in Thermal Analysis
The DSC 404 F1 Pegasus® High-Temperature Differential Scanning Calorimeter, is designed for the exact determination of specific heat of high-performance materials at high temperatures.
- Determination of thermodynamic properties of ceramics and metallic high-performance materials
- Performance of quantitative enthalpy and cp determinations in a pure gas atmosphere
- Vacuum-tight up to 10-4 mbar for creation of highly pure atmospheres for tests on materials sensitive to oxidation
- Characterization of amorphous metals, shape memory alloys and inorganic glasses
This DSC 404 F1 Pegasus® stands for highest flexibility, excellent quality and optimal performance.
The DSC 404 F1 Pegasus® comprises a high-capacity heat flux DSC for highly sophisticated application measurements.
The concept of the DSC 404 F1 Pegasus® allows configuration for up to eight different furnace types, easily interchangeable by the user, for a wide temperature range within -150°C to 2000°C.
We offer diverse sensors for DSC and DTA measurements, various crucible types as well as a great variety of technical accessories.
The coupling to a FT-IR or MS is possible without problems.
An important hardware extension, like the automatic sample changer (ASC) for up to 20 sample and reference crucibles, and software features, such as BeFlat® for an optimized baseline or the optional temperature modulation of the DSC signal (TM-DSC) make the DSC 404 F1 Pegasus® the most versatile DSC system for research & development, quality assurance, failure analysis and process optimization.
The DSC 404 F1 Pegasus® is the ideal tool for your daily laboratory work.... Read More | Fascinating Flexibility in Thermal Analysis
The DSC 404 F3 Pegasus®, High-Temperature Differential Scanning Calorimeter, is part of the economical NETZSCH F3-product line, which is specially tailored to the requirements of comparative material characterization and quality control.
DSC 404 F3 Fascinating Flexibility in Thermal Analysis
The DSC 404 F3 Pegasus®, High-Temperature Differential Scanning Calorimeter, is part of the economical NETZSCH F3-product line, which is specially tailored to the requirements of comparative material characterization and quality control.
DSC 404 F3 Pegasus®, High-Temperature Differential Scanning Calorimeter, can be operated from -150°C to 2000°C with various DTA and DSC sensors that are easily exchangeable by the user and various furnace types (please see accessories).
The sample chamber can be purged with inert or oxidizing gases in order to remove gases evolved from the sample.
The measuring system is vacuum tight (10-4 mbar).... Read More |